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The target product ions were determined as m/z 250.10 for SAM (CE 15 V), m/z 136.05 for SAH (CE 20 V) from the precursor ions of [M + H] + ( m / z 399 for SAM, m/z 385 for SAH)

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GSH (100 gmL 1 ) was incubated at 37 C with the above conditions for 24 h or until at least 20% of peptide was degraded