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Intensity ratios between the paramagnetic and diamagnetic states were computed for all assigned and non-overlapping 1 H, 15 N, and 1 H, 13 C HSQC cross-peaks, employing a correlation time of the electron-spin interaction vector of 4 ns 52,53

Table 1: Gradient Conditions Initial rates of the clearance of test compounds were calculated using linear regression of semi-log plot of % remaining of compounds versus time